Experimental Organic Chemistry: Laboratory ManualAcademic Press, 30.10.2015 - 500 sivua Experimental Organic Chemistry: Laboratory Manual is designed as a primer to initiate students in Organic Chemistry laboratory work. Organic Chemistry is an eminently experimental science that is based on a well-established theoretical framework where the basic aspects are well established but at the same time are under constant development. Therefore, it is essential for future professionals to develop a strong background in the laboratory as soon as possible, forming good habits from the outset and developing the necessary skills to address the challenges of the experimental work. This book is divided into three parts. In the first, safety issues in laboratories are addressed, offering tips for keeping laboratory notebooks. In the second, the material, the main basic laboratory procedures, preparation of samples for different spectroscopic techniques, Microscale, Green Chemistry, and qualitative organic analysis are described. The third part consists of a collection of 84 experiments, divided into 5 modules and arranged according to complexity. The last two chapters are devoted to the practices at Microscale Synthesis and Green Chemistry, seeking alternatives to traditional Organic Chemistry. - Organizes lab course coverage in a logical and useful way - Features a valuable chapter on Green Chemistry Experiments - Includes 84 experiments arranged according to increasing complexity |
Sisältö
| 1 | |
| 29 | |
| 45 | |
Basic Laboratory Operations | 71 |
Determining Physical and Spectroscopic Properties | 145 |
FunctionalGroup Analysis | 177 |
Basic Operation Experiments | 207 |
Organic Synthesis Experiments | 239 |
Advanced Organic Synthesis Experiments | 291 |
Microscale | 353 |
Microscale Experiments | 371 |
Green Chemistry | 409 |
Green Chemistry Experiments | 417 |
| 485 | |
Back Cover | 489 |
Muita painoksia - Näytä kaikki
Experimental Organic Chemistry: Laboratory Manual Joaquín Isac-García,José A. Dobado,Francisco G. Calvo-Flores,Henar Martínez-García Esikatselu ei käytettävissä - 2015 |
Yleiset termit ja lausekkeet
1-bromobutane acetic anhydride acetone alcohol amine anhydrous aqueous aromatic Basic lab operations beaker benzaldehyde brevity calculate the yield carbonyl clamp Compound Mw conical vial container crystals cyclohexene Data Sheet MSDS Density Danger diethyl ether Difficulty Basic lab dissolved dropwise eluent Erlenmeyer flask ester Estimated Difficulty Basic ethyl acetate EtOH experiment Figure filter GHS icons glass Goal Gravity filtration Green Chemistry groups heat Hirsch funnel ice bath icons are indicated inert information offered ketone liquid Liquid-liquid extraction magnetic stirring Material Safety Data MeOH Microscale ml of water ml round-bottom flask mmol molecules MSDS NaOH Non-hazardous Noticeboard Organic Chemistry organic layer organic solvent oxidation Pasteur pipette Physico-chemical properties Procedure reaction crude reagents Recrystallization remove rotary evaporator round-bottom flask Safety Data Sheet sample separatory funnel simple distillation sodium solid soluble solution substance synthesis temperature test tube transfer Vacuum filtration wash weigh Μω
